A new study published in the Journal of Chromatography A presents metabolite profiling of tea (Camella sinensis) harvested from the Bulang Mountains in Yunnan, China, using multidimensional gas chromatography–mass spectrometry (GC×GC–MS) to determine the impact of seasonal changes.
A new study published in the Journal of Chromatography A presents metabolite profiling of tea (Camella sinensis) harvested from the Bulang Mountains in Yunnan, China, using multidimensional gas chromatography–mass spectrometry (GC×GC–MS) to determine the impact of seasonal changes.1
The Yunnan Province in China is a major tea producing area that is affected by the East Asian Monsoon season and is therefore vulnerable to the effects of climate change. Compared to historical records, the East Asian Monsoon now begins earlier and lasts longer in the Yunnan Province than in the past, shortening the optimum harvest period. Tea typically needs 1500–1800 mm of rainfall annually and is harvested seasonally. During the monsoon season, the price of tea harvested can drop by up to 30% because of a decrease in flavour attributed to increasing rainfall. The study authors have previously found that the concentration of catechin and methylaxanthine can drop by more than 50% from the spring to the monsoon season.2
Tea leaves were sampled from three areas at elevations between 1600 m and 1850 m in the Bulang Mountains over 18 days during the spring and monsoon season in 2012. Samples were then extracted and analyzed using automated sequential GC×GC–MS. The authors reported that 201 spring metabolites and 196 monsoon metabolites were identified, of which 59 were seasonally unique compounds. - B.D.
References
1. A. Kowalsick et al., Journal of Chromatography A 1370, 230–239 (2014).
2. S. Ahmed et al., PLoS ONE9, e109126 (2014).
This story originally appeared in The Column. Click here to view that issue.
Analytical Challenges in Measuring Migration from Food Contact Materials
November 2nd 2015Food contact materials contain low molecular weight additives and processing aids which can migrate into foods leading to trace levels of contamination. Food safety is ensured through regulations, comprising compositional controls and migration limits, which present a significant analytical challenge to the food industry to ensure compliance and demonstrate due diligence. Of the various analytical approaches, LC-MS/MS has proved to be an essential tool in monitoring migration of target compounds into foods, and more sophisticated approaches such as LC-high resolution MS (Orbitrap) are being increasingly used for untargeted analysis to monitor non-intentionally added substances. This podcast will provide an overview to this area, illustrated with various applications showing current approaches being employed.
Using Chromatography to Study Microplastics in Food: An Interview with Jose Bernal
December 16th 2024LCGC International sat down with Jose Bernal to discuss his latest research in using pyrolysis gas chromatography–mass spectrometry (Py-GC–MS) and other chromatographic techniques in studying microplastics in food analysis.
The Use of SPME and GC×GC in Food Analysis: An Interview with Giorgia Purcaro
December 16th 2024LCGC International sat down with Giorgia Purcaro of the University of Liege to discuss the impact that solid-phase microextraction (SPME) and comprehensive multidimensional gas chromatography (GC×GC) is having on food analysis.