Researchers Discover Tuberculosis in 9,000-year-old skeleton using HPLC
October 15th 2008Research by scientists from University College London (UCL) and Tel Aviv University shows that the tuberculosis infection is 3,000 years older than was previously imagined and that TB in people evolved before bovine TB.
Weed Killer Analyzed Using Molecularly Imprinted Polymer
October 15th 2008A research group from BRGM (Orleans, France) and Ecole Superieure de Physique et de Chimie Industrielles (Paris, France) used terbutylazine molecularly imprinted polymers following a pressurized liquid extraction step to remove interfering compounds from soil extracts containing the herbicide atrazine.
Stoichiometrically Imprinted Polymer SPE of Fluoroquinolones
October 15th 2008Researchers from Universidad Complutense de Madrid (Madrid, Spain) and Universität Dortmund (Dortmund, Germany) used a molecularly imprinted polymer (MIP) solid-phase extraction method in the analysis of fluoroquinolone antibiotics in environmental water samples.
Monolithic Spin Column Extraction of Amphetamines
October 15th 2008Researchers from Hiroshima University (Hiroshima, Japan), Hiroshima Prefectural Police Headquarters (Hiroshima), Tokai University School of Medicine (Kanagawa, Japan), and GL Sciences Inc. (Saitama, Japan) developed a spin column device packed with octadecyl silane-bonded monolithic silica for extracting amphetamines and methylenedioxyamphetamines from urine.
Thermo Fisher Scientific LC-MS-MS System Used to Detect Melamine
October 15th 2008Thermo Fisher Scientific (San Jose, California) announced that a method that uses the company?s equipment for detecting melamine and cyanuric acid in food matrixes was described in the U.S. FDA?s Laboratory Information Bulletin Number 4396, May 2007.
Waters Joins Microsoft's BioIT Alliance
October 15th 2008Waters Corporation (Milford, Massachusetts) has joined the BioIT Alliance, an initiative spearheaded by Microsoft Corporation (Redmond, Washington) that involves more than 80 pharmaceutical, biotech, laboratory instrument, and software companies working together to advance personalized medicine.
SBSE Used in Triclosan Analysis
October 15th 2008Scientists from Hoshi University (Tokyo, Japan) and the National Research Institute of Police Science (Chiba, Japan) employed stir-bar sorptive extraction (SBSE) and thermal desorption gas chromatography?mass spectrometry (GC?MS) for analyzing 5-chloro-2-(2,4-dichlorophenoxy)phenol, otherwise known as triclosan, in river water samples.
Thermo Fisher serve up food and drink at show
October 10th 2008Thermo Fisher Scientific showcased its comprehensive laboratory instrumentation and informatics solutions for food, beverage and agricultural applications at the 2008 Association of Analytical Communities (AOAC) annual meeting and exposition at the end of September...
Ask the Editor: Method Development
October 8th 2008The following question and answer were taken from LCGC Europe's "CE Currents" column (1). How should I approach method development? If possible request any details of sample stability, pKa, and solubility in different solvents and pH ranges. Information on solvents used in HPLC can also be useful.
Quick and Easy Membrane Characterization with Size Exclusion Chromatography
October 6th 2008Size exclusion chromatography (SEC) is a powerful tool for the characterization of molecules differing in size and molar mass. It is widely used and well known for the determination of molar mass distributions and molar mass averages. For membranes GPC/SEC is a useful characterization method as it can measure the membrane characteristic pore size distribution, average pore size and molecular cut-off significantly faster than other methods.
Fast Gradient LC Using Your Existing Instrumentation
October 6th 2008Transforming "standard" gradient HPLC systems into extremely fast gradient systems is readily achievable with proper application of chromatographic principles, particularly temperature control, combined with utilization of advanced HPLC columns. Bottom line: You don't have to buy a new LC to achieve ultra high quality and speed!