Evaluating Marine Algae for Therapeutic Effects
May 15th 2018Snezana Agatonovic-Kustrin, a professor in pharmaceutical chemistry at Monash University, in Kuala Lumpur, Malaysia, spoke to The Column about the development of a method to evaluate antidiabetic and antioxidant activity in marine algae using high-performance thin-layer chromatography (HPTLC)-direct bioautography.
Novel Methods Using Mass Spectrometry for Food Safety—From Contamination to Nutrition
May 15th 2018This article highlights three events that require new method development to meet various detection needs, ranging from the detection of pesticides such as fipronil and glyphosate, to the detection and quantification of fat-soluble vitamins.
The LCGC Blog: Problems and Ionic Liquid Solutions for Soil BTEX Analysis
May 15th 2018I do not remember the application, but I remember very clearly Professor McNair telling us that soil is one of the most challenging sample matrices, if not the toughest, from which to perform analytical determinations. Sources indicate the composition of soil ideal for growing plants to be 25% air, 25% water, 45% minerals, and 5% organic matter. That does not seem like a daunting makeup, but the reality is that the relative proportion of the constituents can vary dramatically.
Modern PFAS Analysis: New Analytical Options for Testing PFAS in Various Matrices
May 15th 2018Per- and polyfuorinated alkyl substances (PFAS) are a rapidly growing environmental and human health concern. Owing to their broad commercial use, chemical stability, and bioaccumulation potential, these compounds are widely dispersed in the environment and can cause exposure through many potential pathways. To adequately estimate exposure risks, analytical methods are required that can measure low levels of PFAS compounds in many types of matrices. As will be described, recent advances in solid-phase extraction (SPE) and liquid chromatography tandem mass spectrometry (LC–MS/MS) have enabled the identification and quantification of a large number of PFAS compounds at low concentration (
Determination of Organometal Contaminants Using PTV GC–ICP-MS
May 15th 2018Researchers from the Université de Pau et des Pays de l’Adour, in France, have developed a large volume injection method using a programmed temperature vaporization (PTV) injector for the simultaneous determination of mercury, tin, and lead at ultra-trace levels in natural waters using GC–ICP-MS.