Patrick Lavery is an Editor for the MJH Life Sciences brands LCGC and Spectroscopy, and their respective websites, chromatographyonline.com and spectroscopyonline.com. He previously spent nearly a decade as a news anchor, reporter, and producer at New Jersey 101.5 FM.
LC–MS/MS Helps Detect ε-(γ-glutamyl) Lysine as Transglutaminase 2 Biomarker in Human Urine
May 19th 2023A biomarker with significant clinical and analytical potential in an enzyme present in many human diseases was determined at higher efficiency using liquid chromatography coupled to tandem mass spectrometry (LC–MS/MS).
Novel Approach to Perfectly Ordered Chromatographic Columns Uses Structured Microgroove Arrays
May 8th 2023A newly proposed concept in liquid chromatography (LC) positions spherical particles, either individually or stacked, in pockets forming microgrooves that act as perfectly aligned chromatographic columns.
SPME Arrow Improves Upon Conventional SPME in GC×GC–MS Analysis of Whiskey Flavor Compounds
May 5th 2023A solid-phase microextraction (SPME) Arrow combined with comprehensive two-dimensional gas chromatography coupled to mass spectrometry (GC×GC–MS) identified about 40 more volatile compounds in a variety of whiskeys compared to conventional SPME.
New SBSE–HPLC-DAD Method Proposed to Analyze Trace PCBs in Environmental Waters
May 3rd 2023Trace amounts of polychlorinated biphenyls (PCBs) in a river and lake in China were detected using a custom coating for stir bar sorptive extraction (SBSE) followed by high performance liquid chromatography with diode array detection (HPLC-DAD).
GC✕GC–TOF-MS Used with F-ratio Analysis to Evaluate Volatiles in Getter Substrate Breakdown
May 2nd 2023Researchers have used comprehensive two-dimensional gas chromatography with time of flight mass spectrometry and Fisher-ratio analysis to evaluate the breakdown of organic-based getters used to absorb gases and vapors from their surroundings.
New Extraction Approach Combined with HPLC-UV to Monitor Chloramphenicol in Milk and Chicken
May 2nd 2023Researchers have developed a new approach to extract chloramphenicol (CAP) from milk and chicken samples using magnetic nanofluid-based deep eutectic solvents (DES), which was combined with high performance liquid chromatography-ultraviolet (HPLC-UV) analysis. The method was found to be low-cost, green, efficient, and effective in detecting even trace amounts of CAP.
Using HPLC–MS and GC–MS for Improving Speed and Accuracy of Organosulfur Compound Detection
May 2nd 2023High performance liquid chromatography–mass spectrometry and gas chromatography–mass spectrometry, along with numerous extraction methods, are helping to find organosulfur compounds in food more easily, providing researchers better information about the health benefits of these substances.
GC✕GC–TOF-MS Helps Quantify Pesticides in Water Susceptible to Contamination
April 28th 2023Pesticides in local surface and groundwaters were purified and enriched with solid-phase extraction, then analyzed using multidimensional gas chromatography coupled to mass spectrometry, with the results compared to those found by gas chromatography–quadrupole mass spectrometry.