GC-MS Method Developed to Identify Oils and Oil Binders in Paintings
A GC-MS procedure has been developed, optimized, and applied to characterization of oil binders in paintings.
A GC-MS procedure has been developed, optimized, and applied to characterization of oil binders in paintings. The procedure involves hydrolysis of lipids to fatty acids (FAs) and derivatization of FAs to fatty acid methyl esters (FAMEs). FAMEs are analyzed by temperature-programed GC followed by full-scan MS. The method provides a good repeatability of results and has been applied to the characterization of common plant oils used in paintings, commercial oil and tempera paints, model painting samples, and to samples taken from real paintings.
Miniaturized GC–MS Method for BVOC Analysis of Spanish Trees
April 16th 2025University of Valladolid scientists used a miniaturized method for analyzing biogenic volatile organic compounds (BVOCs) emitted by tree species, using headspace solid-phase microextraction coupled with gas chromatography and quadrupole time-of-flight mass spectrometry (HS-SPME-GC–QTOF-MS) has been developed.
Fundamentals of Benchtop GC–MS Data Analysis and Terminology
April 5th 2025In this installment, we will review the fundamental terminology and data analysis principles in benchtop GC–MS. We will compare the three modes of analysis—full scan, extracted ion chromatograms, and selected ion monitoring—and see how each is used for quantitative and quantitative analysis.
Quantifying Microplastics in Meconium Samples Using Pyrolysis–GC-MS
March 26th 2025Using pyrolysis-gas chromatography and mass spectrometry, scientists from Fudan University and the Putuo District Center for Disease Control and Prevention detected and quantified microplastics in newborn stool samples.
The Role of SPME Combined with GC–MS for PFAS Analysis
Published: March 25th 2025 | Updated: March 25th 2025Emanuela Gionfriddo and Madison Williams from University at Buffalo, the State University of New York, NY, USA discuss the important role that solid-phase microextraction (SPME) techniques with gas chromatography mass spectrometry (GC–MS) can play in the analysis of per- and polyfluoroalkyl substances (PFAS).
