A GC-MS procedure has been developed, optimized, and applied to characterization of oil binders in paintings.
A GC-MS procedure has been developed, optimized, and applied to characterization of oil binders in paintings. The procedure involves hydrolysis of lipids to fatty acids (FAs) and derivatization of FAs to fatty acid methyl esters (FAMEs). FAMEs are analyzed by temperature-programed GC followed by full-scan MS. The method provides a good repeatability of results and has been applied to the characterization of common plant oils used in paintings, commercial oil and tempera paints, model painting samples, and to samples taken from real paintings.
Analysis of Pesticides in Foods Using GC–MS/MS: An Interview with José Fernando Huertas-Pérez
December 16th 2024In this LCGC International interview with José Fernando Huertas-Pérez who is a specialist in chemical contaminants analytics and mitigation at the Nestlé Institute for Food Safety and Analytical Sciences at Nestlé Research in Switzerland, In this interview we discuss his recent research work published in Food Chemistry on the subject of a method for quantifying multi-residue pesticides in food matrices using gas chromatography–tandem mass spectrometry (GC–MS/MS) (1).
Using Chromatography to Study Microplastics in Food: An Interview with Jose Bernal
December 16th 2024LCGC International sat down with Jose Bernal to discuss his latest research in using pyrolysis gas chromatography–mass spectrometry (Py-GC–MS) and other chromatographic techniques in studying microplastics in food analysis.