This Tuesday afternoon session will discuss mass spectrometry analysis of emerging environmental contaminants found in fish, wastewater effluent, arctic snow, drinking water, and other matrices. It will be chaired by Eunha Hoh of San Diego State University and will be held in Ballroom 6A from 2:30 to 4:30 p.m.
This Tuesday afternoon session will discuss mass spectrometry analysis of emerging environmental contaminants found in fish, wastewater effluent, arctic snow, drinking water, and other matrices. It will be chaired by Eunha Hoh of San Diego State University and will be held in Ballroom 6A from 2:30 to 4:30 p.m.
Jonathan Mosley of US EPA in Athens, Georgia will lead off this session with a talk titled “High-Resolution Mass Spectrometry of Skin Mucus for Monitoring Physiological Impacts and Biotransformation Products in Fish Exposed to Wastewater Effluent.” His talk will discuss an MS-based untargeted metabolomics approach that led to the discovery of contaminant biotransformation products on the skin of exposed fish.
Next, Hailemariam Assress of the University of South Africa (Johannesburg) will present a talk titled “Retrospective Suspect and Non-Target Screening of Emerging Pollutants and Transformation Products in Wastewater Effluent Using UHPLC-QTOF-MS/MS.” This presentation will describe a screening approach for pollutants in wastewater effluent previously generated for target analysis without the need for reinjection of water samples.
Judy Westrick of Wayne State University (Detroit, Michigan) will then present a talk titled “Using Mass Spectrometry to Vet Cyanotoxin Concentrations by Enzyme-Linked Immunosorbent Assay (ELISA).” In this study, targeted and untargeted workflows for microcystin MS were used to evaluate the ELISA method.
The next presentation, titled “Organic Pollutants in the Snow of Russian Arctic Islands: 2016-2017 Expeditions,” will be given by Dmitrii Mazur of Moscow State University (Moscow, Russia). Mazur’s presentation will discuss the non-targeted analysis of semivolatile organic compounds in snow samples from the Novaya Zemlya archipelago.
Hannah Liberatore of the University of South Carolina will present the next talk, “Energy Extraction and Utilization Impacts on Drinking Water Disinfection By-Product Formation and Toxicity.” She will describe an investigation of disinfection by-products from bromide, iodide, and organic precursors contributed by hydraulic fracturing and coal-fired power plant wastewaters during drinking water disinfection.
The final presentation in the session will be given by Amy McKenna of the National High Magnetic Field Laboratory in Tallahassee, Florida, and is titled “Targeted Analysis of Oxygen Transformation Products Derived from Weathered Oil by FT-ICR MS.” Her talk will discuss a comparison of heavily weathered oil residues that highlights the molecular signature of oxygenated transformation compounds of different chemical functionalities.
SPE-Based Method for Detecting Harmful Textile Residues
January 14th 2025University of Valencia scientists recently developed a method using solid-phase extraction (SPE) followed by high-performance liquid chromatography coupled to high-resolution mass spectrometry (HPLC–HRMS/MS) for detecting microplastics and other harmful substances in textiles.
The Complexity of Oligonucleotide Separations
January 9th 2025Peter Pellegrinelli, Applications Specialist at Advanced Materials Technology (AMT) explains the complexity of oligonucleotide separations due to the unique chemical properties of these molecules. Issues such as varying length, sequence complexity, and hydrophilic-hydrophobic characteristics make efficient separations difficult. Separation scientists are addressing these challenges by modifying mobile phase compositions, using varying ion-pairing reagents, and exploring alternative separation modes like HILIC and ion-exchange chromatography. Due to these complexities, AMT has introduced the HALO® OLIGO column, which offers high-resolution, fast separations through its innovative Fused-Core® technology and high pH stability. Alongside explaining the new column, Peter looks to the future of these separations and what is next to come.