SBSE in the Analysis of Pharmaceuticals in Water
A research group from the University of Lisbon (Lisbon, Portugal) studied the use of stir-bar sorptive extraction (SBSE) with polyurethane and polydimethylsiloxane polymeric phases and high performance liquid chromatography with diode-array detection for the analysis of six acidic pharmaceutical compounds in environmental water matrices such as river, sea, and wastewater samples.
A research group from the University of Lisbon (Lisbon, Portugal) studied the use of stir-bar sorptive extraction (SBSE) with polyurethane and polydimethylsiloxane polymeric phases and high performance liquid chromatography with diode-array detection for the analysis of six acidic pharmaceutical compounds in environmental water matrices such as river, sea, and wastewater samples. The compounds of interest were o-acetylsalicylic acid, ibuprofen, diclofenac sodium, naproxen, mefenamic acid, and gemfibrozil. In this study, the polyurethane phase was found to be more effective at extracting the analytes from the water matrices.
Common Challenges in Nitrosamine Analysis: An LCGC International Peer Exchange
April 15th 2025A recent roundtable discussion featuring Aloka Srinivasan of Raaha, Mayank Bhanti of the United States Pharmacopeia (USP), and Amber Burch of Purisys discussed the challenges surrounding nitrosamine analysis in pharmaceuticals.
Extracting Estrogenic Hormones Using Rotating Disk and Modified Clays
April 14th 2025University of Caldas and University of Chile researchers extracted estrogenic hormones from wastewater samples using rotating disk sorption extraction. After extraction, the concentrated analytes were measured using liquid chromatography coupled with photodiode array detection (HPLC-PDA).
