GC–MS

Webinar Date/Time: Tuesday, May 28, 2024 Airing 1: 11am EDT | 8am PDT | 10am CET | 4pm SGT Airing 2: 2pm EDT | 11am PDT | 1pm CET | 7pm SGT

Webinar Date/Time: Wed, May 15, 2024 2:00 PM EDT

Chromatographic and spectroscopic techniques alike were reviewed for their current effectiveness and future potential in this lecture session at Analytica 2024.

Here are the top five articles that the editors of LCGC International published this week.

Adopted 35 years ago, the Montreal Protocol is an international treaty designed to protect the ozone layer. It addresses ozone depletion caused by industrial chemicals and remains a landmark environmental agreement in the phasing out and ban of the production and consumption of ozone-depleting substances (ODSs).

A study has used gas chromatography coupled to a time-of-flight mass spectrometer to build an electron ionization mass spectra database of more than 250 chemicals classified as either volatile or semi-volatile compounds. An additional, confirmatory layer of liquid chromatography–mass spectrometry analysis was subsequently performed.

Element Materials Technology introduced its Rapid Response Pharmaceutical Testing Service, providing expedited testing and focusing on various requirements including active ingredients and final drug products, extractables and leachables, degradation production, and elemental impurities.

A study has proposed targeted methods, developed using gas chromatography coupled to tandem mass spectrometry, to measure human plasma protein binding and hepatocyte clearance in 73 per- and polyfluoroalkyl substances, or PFAS.

Limited toxicokinetic and toxicologic information is available about a diverse set of per- and polyfluoroalkyl substances (PFAS), but methods based on gas chromatography–tandem mass spectrometry (GC–MS/MS) can help unravel some of the mystery.

The company’s new service will provide expedited testing to customer around the world.

This week, LCGC International published a variety of articles on the hottest topics in chromatography and beyond. Below, we’ve highlighted some of the most popular articles, according to our readers. Happy reading!

In this edition of “Inside the Laboratory,” Kevin Schug, PhD, a full professor of chemistry at the University of Texas at Arlington, discusses his laboratory’s group work in environmental monitoring around water and soil quality near oil and gas extraction, using techniques such as liquid chromatography (LC), gas chromatography (GC), supercritical fluid chromatography (SFC), and coupling these techniques with mass spectrometry (MS).

Scientists investigated using this method to measure volatile organic compounds in the breath of patients with chronic kidney disease.

Webinar Date/Time: Wed, Apr 10, 2024 10:00 AM EDT

Researchers from Austria, Greece, and Italy conducted a study to analyze volatile organic compounds (VOCs) present in Irish and Scotch whiskys using solid-phase microextraction (SPME) Arrow with comprehensive two-dimensional gas chromatography coupled to mass spectrometry (GC×GC–MS) to examine the organoleptic characteristics that influence the taste of spirits.

A recent study from the Cantonal Laboratory Zürich examined using micro solid-phase extraction for pesticide analysis.

A recent study explores the use of liquid–liquid extraction (LLE) and gas chromatography–mass spectrometry (GC–MS) to identify the compounds found in extractives of Alaska Yellow Cedar trees.

A group of Taiwanese scientists have recently created a new method for assessing food quality and detecting histamine in wine samples.

Webinar Date/Time: Tuesday and Wednesday, March 26 and 27, 2024 Morning Session: 9:30am - 12:00pm EDT Afternoon Session: 2:00pm - 4:00pm EDT

During a workshop at Pittcon, David Alonso of LECO Corporation discussed how gas chromatography–time-of-flight mass spectrometry (GC-TOFMS) can be used to identify polyfluorinated alkyl chemicals (PFAS) chemicals in anti-fog product solutions.

A recent study from the United Kingdom Centre for Ecology & Hydrology shows how gas chromatography–mass spectrometry can be used to detect 6PPD, a common additive used in the production of car tires, in water environments to combat environmental pollution.

A research collaboration between researchers from Denmark and Brazil used gas chromatography–mass spectrometry (GC–MS) to determine levels of taste and odor compounds in Nile tilapia.

A new method has been developed to provide a sensitive, accurate and convenient GC–MS method to align with the new European regulation in relation to the introduction of the new Accutrace Plus marker for fuels.

The 18th International Symposium on Hyphenated Techniques in Chromatography and Separation Technology will take place from 28–31 May 2024 in Leuven, Belgium.

Blood and sputum are the most common means of detection by diagnostic tests, but producing adequate sputum can be difficult given a dry cough is often a TB symptom.

Researchers employed advanced chromatography and mass spectrometry techniques to unravel the chemical components and metabolites of Lingbao Huxin Dan, pinpointing its therapeutic potential for cardiovascular ailments.

Researchers at Agro Innovation International in France have employed the HS-SPME-GC–MS technique to characterize volatile organic compounds (VOCs) in farm effluents, presenting a simple, fast, and economical method for quantifying 177 and 77 VOCs in laboratory and field tests, respectively, providing valuable insights for monitoring olfactory nuisances and predicting effluent material evolution.

A polydimethylsiloxane (PDMS) silicone rubber band sampler was used to collect volatile organic compounds (VOCs) from the skin of both tuberculosis (TB)-positive and TB-negative subjects.

Non-alcoholic beers are becoming more popular and need to reflect the sophisticated flavourings of beers that are brewed containing alcohol. Sophisticated analytical techniques can help to achieve this.

Alena Kubatova, a professor in the Department of Chemistry at the University of North Dakota, in Grand Forks, North Dakota, is exploring new approaches in characterizing lignin, to understand its structural complexities and how these methods can help improve processing in biorefineries. LCGC spoke to Kubatova to discuss her recent research in understanding the chemistry of lignin.